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Jiangsu Skyray Instrument Co., Ltd.
Shenzhen Skyray Instrument Co., Ltd.

TEL86 136 1622 3382

hotline800-9993-818

addressNo. 1888, Zhonghuayuan West Road, Kunshan City, Jiangsu Province, 22/F, Taohuayuan Science and Technology Innovation Park, Furong East Road, Songgang, Bao'an District, Shenzhen, China

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Jiangsu Skyray Instrument Co., Ltd.-GC-MS6800 Detection of Phthalates in Electronic Information Products...

ROHS2.0Halogen-free detection analyzer

GC-MS6800 Detection of Phthalates in Electronic Information ...

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  800-9993-818
  86 136 1622 3382

 GC-MS6800 Detection of Phthalates in Electronic Information Products...  Product Details

GC-MS 6800是天瑞仪器精心打造的一款高性价比气相色谱质谱联用仪,具有完全的自主知识产权,拥有多项专利技术,可广泛应用于工业检测、食品安全、环境保护等众多领域。


技术优势

硬件

自主研发的GC系统,带电子流量和电子压力控制(EFC、EPC)
自主研发高效灯丝,电子发射效率高,最大可达350μA
带预四极的单四极杆质量分析器,有效减少测样过程对四极杆的污染;
带高能转换打拿极的电子倍增器提供优秀的灵敏度;
进口机械泵和分子泵组成优异的真空系统,保证系统的高稳定性和可靠性;
配备全量程真空规,实时监测真空状况;
完善的保护系统,保证仪器出现异常状况时保护系统关键部件,延长仪器使用寿命;
先进的RF电源数字补偿技术,可以使全质量范围内的质谱峰都达到较高的灵敏度和分辨率;

软件

工作站软件可同时控制气相色谱仪、自动进样器和质谱仪,通过高速网卡实现数据采集与传输;
支持全扫描(FULL SCAN)和选择离子扫描(SIM)模式;
可实现FULL SCAN、SIM扫描;
支持手动调谐和自动调谐;
实时显示总离子流谱和质谱图谱;
可快速提取离子和全扫描图谱;
天瑞仪器是NIST授权的国内唯一合法分销商,可以保证用户得到最新的NIST谱库数据和谱库升级功能;
数据处理软件可依据样品的质谱图在NIST2011谱库中进行目标化合物自动搜寻,并显示搜寻结果。搜寻结果显示每个化合物的实测保留时间、分子结构式与标准图谱,确认离子之间的标准丰度比与实测丰度比等以供使用者准确定性、定量分析;

国际级的品质:核心部件与国际主流产品保持一致,保证了GC-MS6800具备与国外仪器同样的性能品质
满足更多需求:天瑞仪器为客户提供多种性能优良的选配件,满足不同领域不同客户的多种需求
人性化设计: 整机的人性化设计,不仅方便操作,也为让日常维护更加轻松
离子化效率更高:整机模块化设计,并采用天瑞专利-新型离子源,离子化效率更高,达到整机灵敏度大大提高
Chem Analyst色质联用工作站:实现高效、快速、多功能仪器控制、数据采集、数据处理
超高的性价比:在满足全部应用需求的情况下,天瑞为客户带来了更多的实惠
科学的解决方案:天瑞仪器强大的应用研发中心为客户提供全面的应用分析解决方案,让客户体验到量身打造的舒适
优惠的耗材价格:灯丝等耗材和配件自主研发,客户在享受高端性能的同时,还可以在仪器维护上节省一笔不小的开支
完善的售后服务:天瑞仪器对客户需求响应快速,专业技术人员24小时全天候服务

应用领域

1、工业领域:纺织,电子电器,塑胶,化妆品
2、食品安全:农药残留,香精香料,添加剂,包装材料
3、环境保护:大气,水质,土壤,固体废弃物
4、生物医药:制药厂,药物检测
5、石油化工:炼油厂,化工厂
6、公检法系统:刑侦,爆炸物,毒品分析,鉴定物证


201616日,由工业和信息化部、发展改革委、科技部、财政部、环保部、商务部等八部门联合公布了《电器电子产品有害物质限制使用管理办法》[1](第32号令,即中国RoHS2.0),并于201671日正式实施;相对于2006年实施的《电子信息产品污染控制管理办法》(也称中国RoHS1.0),新版RoHS2.0在适用范围、限制使用有害物质管理方式等方面做了重大调整,具体如下:

序号

主要修订

修订内容解析

1

扩大规章的适用范围并修改规章名称

将调整对象由电子信息产品扩大为电器电子产品,并将规章名称修改为《电器电子产品有害物质限制使用管理办法》。同时,《办法》对电器电子产品的含义做出了规定。

2

扩大限制使用的有害物质范围

借鉴欧盟RoHS指令和其他国家的通行做法,增加了限制使用的有害物质,将“铅”、“汞”、“镉”分别修改为“铅及其化合物”、“汞及其化合物”、“镉及其化合物”,将“六价铬”修改为“六价铬化合物”。

3

增加有关科技、财政政策支持的规定

新版RoHS规定:国家鼓励、支持电器电子产品有害物质限制使用的科学研究、技术开发和国际合作,积极推广电器电子产品有害物质替代与减量化等技术、装备。

4

完善产品有害物质限制使用的管理方式

电器电子产品有害物质限制使用采取目录管理的方式,由工信部商发展改革委等7部门编制“达标管理目录”,不再编制“重点管理目录”。同时,建立合格评定制度,对纳入“达标管理目录”的电器电子产品按照合格评定制度进行管理。合格评定制度由认监委依据工业和信息化部的建议并会同工业和信息化部制定。工业和信息化部根据实际情况会同财政部等部门对合格评定结果建立相关采信机制。

  新版RoHS 2.0的适用范围扩大为电器电子产品,几乎涵盖了所有家电产品,并且对进出口产品与国产一视同仁,具体涉及限制物质清单如下:

序号

物质名称

限量要求

1

铅及其化合物

0.1%

2

汞及其化合物

0.1%

3

镉及其化合物

0.01%

4

六价铬化合物

0.1%

5

多溴联苯(PBB

0.1%

6

多溴二苯醚(PBDE

0.1%

7

国家规定的其他有害物质


 

     针对以上限制物质清单的检测,《GB/T 26125-2011 电子电气产品 六种限制物质的测定》[2]指定了上述有害物质的检测手段和方法,天瑞仪器的气相色谱质谱联用仪(GC-MS 6800)可用于新版RoHS2.0中多溴联苯和多溴二苯醚的定量分析。

GC-MS 6800仪器简介

GC-MS 6800用于有机物的检测,是挥发性和半挥发性定性定量分析测试的常见方法,广泛应用于各种有机毒害物的残留分析项目,具有检出限低,定性能力强,定量结果准确等特点,可有效地应用于中国RoHS 2.0中多溴联苯和多溴二苯醚的定性和定量分析。


测试流程

多溴联苯和多溴二苯醚样品测试流程

参照IEC62321[3] 、GB/Z 21276-2007[4] 等方法,精确称取一定量的样品颗粒,经溶剂提取→浓缩→净化→定容→过滤,即可上机测试。

以下是20种多溴联苯和多溴二苯醚混合标准溶液TIC图:

1、一溴联苯;2、一溴二苯醚;3、二溴联苯;4、二溴二苯醚;5、三溴联苯;6、三溴二苯醚;7、四溴联苯;8、五溴联苯;9、四溴二苯醚;10、六溴联苯;11、五溴二苯醚;12、六溴二苯醚;;13、七溴联苯;14、七溴二苯醚;15、八溴联苯;16、八溴二苯醚;17、九溴联苯;18、九溴二苯醚;19、十溴联苯;20、十溴二苯醚

附:实验室间比对合格证书

 

参考文件:

[1]. 《电器电子产品有害物质限制使用管理办法》

[2]. GB/T 26125-2011 电子电气产品 六种限制物质(铅、汞、镉、六价铬、多溴联苯和多溴二苯醚)的测定》

[3]. IEC 62321 Electrotechnical products – Determination of levels of six regulated substances(lead, mercury, cadmium, hexavalent chromium, polybrominated biphenyls,polybrominated diphenyl ethers)

[4]. 《GB/Z 21276-2007 电子电器产品中限用物质多溴联苯(PBBs)、多溴二苯醚(PBDEs)检测方法》


Why select Skyray Instruments?

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    First, the industry leader:

    Listed on Shenzhen Stock Exchange in 2011(Code:300165)
    Analytical instrument industry leader in the field

    Skyray Instrument, as a leader in the domestic chemical analysis industry, specializes in the production of high-end analytical instruments such as spectrometers, chromatographs, and mass spectrometers. Mainly used in environmental protection and safety (electronics, electricity, toys and other consumer products industries, food safety, air, soil, water quality pollution detection, etc.), industrial production quality control (metallurgy, building materials, petroleum, chemical, precious metals, medical equipment, etc. ), minerals and resources (geology, mining), commodity inspections, quality inspections, and even human trace element testing and many other areas.The core patent technology is the first in the industry; the sales volume is the first in the industry; the product category is the first in the industry;

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Second, the standard makers:

    Skyray Instrument participated in drafting and formulating 18 national standards, Industry standards, confident in the right to speak in the industry.

    GBT 28020-2011 Ornaments Determination of harmful elements X-ray fluorescence spectroscopy
    GBT 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
    GBT 33352-2016 General requirements for screening of restricted substances in electrical and electronic products X-ray fluorescence spectroscopy
    GB/T 25934.1-2010 High-Purity Gold Chemical Analysis Method Ethyl Acetate Extraction Separation ICP-AES Spectrometry Determination of Impurity Elements
    GB/T 27730-2011 Determination of dimethyl fumarate in toy products Gas chromatography-mass spectrometry GC-MS method
    GB/T 28020-2011 articles - Determination of harmful elements - X-ray fluorescence spectrometry
    GBT 22788-2008 Determination of Total Lead in Coatings on Toys
    GB/T 30419-2013 Determination of migrating elements in gallium arsenic, cadmium, chromium, lead, mercury selenium in toy materials Inductively coupled plasma atomic emission spectrometry
    GB/T 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
    JBT 12962.1-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 1: General Techniques
    JBT 12962.2-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 2: Elemental Analyzers
    JBT 12962.3-2016 Energy dispersive X-ray fluorescence spectrometer Part 3: Coating thickness analyzer
    LS_T 6115-2016.4672 LST6115-2016 "Fastness determination of cadmium in rice by X-ray fluorescence spectrometry" standard
    (Unfinished……)

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Third, technology pioneers:

    252 utility patents to fill domestic gaps and break the import monopoly

    As of the end of 2017, Tianrui Instrument Company and its subsidiaries have obtained 252 patents authorized by the State Intellectual Property Office.
    "Computer Software Copyright Registration Certificate" 91 items;
    Of which 115 are invention patents,
    80 utility model patents,
    Appearance patent 57 items.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Fourth, service practitioners:

    Do not forget the initial heart, with the customer with the fate, a total of growth.

    Skyray customers include the General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China and the National Museum of China,
    China National Center for Geoanalysis and Experiments, Chinese Academy of Geological Sciences, Changchun Institute of Opto-Mechanical Engineering, China Taier Laboratory,
    Other government departments and well-known testing agencies,
    And PetroChina, Sinopec, Huawei, Haier, Skyworth, Fanta, Meiling, Lite-On, TCL, LG, Midea, Samsung, China Test (CTI), Avionics, etc.

研发实力:

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Analytical Testing Instrument Research Institute

    Skyray Analytical Testing Instrument Research Institute has three centers, namely "analysis instrument research and development center", "physiochemical analysis and testing center" and "analysis and testing technology application development center."Tianrui Analytical Instruments Co., Ltd. recently formed a staff of 1 academician, 11 Ph.D., 13 senior engineers, 17 masters, and 50 undergraduate R&D personnel from famous universities.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Dr. Liu Zhaogui, specialist in special allowance of the State Council

    Mr. Liu Zhaogui: graduate student in nuclear physics from Tsinghua University. It has been appraised as the outstanding entrepreneur of Jiangsu Province, the young and middle-aged experts who have outstanding contribution in Jiangsu Province, the first science and Technology Minister of Kunshan, and the national science and technology ministry "scientific and technological innovation and entrepreneurial talent". With the approval of the State Council, the special allowance of the State Council is enjoyed.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Dr. Yaodong Dong, Expert in X-Ray Fluorescence Spectroscopy

    Dr. Yao graduated from the Department of Engineering Physics of Tsinghua University with a Ph.D. in nuclear electronics. He has been engaged in the development of analytical instruments for 26 years. He is mainly engaged in the research of X-ray fluorescence analysis technology and application technology, and he participated in the "Thirteenth Five-Year Plan" national key instrument technology research and development. Patent of "Spectrometer Grating 2D" patent, "X-ray fluorescence double crystal fixed element track spectrometer" patent and "X-ray fluorescence spectrum analyzer pyrolytic graphite crystal beam splitter" patent, and participated in the drafting of a number of national standards industry The standard is an authoritative expert in the X-ray fluorescence spectrometer industry in China.

Eight technical advantages:

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    First, FP basic parameter method

    The FP (Basic Parameters) algorithm is an effective method for X-ray fluorescence spectrometry analysis. It can perform qualitative and quantitative analysis of the elemental components of the sample with little or no standard sample, and can also analyze the thickness of the coating or coating.It is well known that the biggest problem with X-ray fluorescence analysis is that elemental fluorescence intensity is affected by coexisting elements (matrix absorption and enhancement effects) and is not usually linear with content. The basic parameter method has already taken into account the matrix effect in the calculation of the spectrum, and the linear relationship between the calculated content and the known content can be obtained. Using a few known sample calibration algorithms to eliminate systematic errors can achieve accurate quantitative results.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Second, polarization secondary target excitation technology

    The polarization secondary target excitation technology can remove the scattering background to the maximum extent, improve the signal to noise ratio, and reduce the detection limit of the detector. Assuming that the x-ray generated by the anode of the x-ray tube is non-polarized and is incident on the target (scattering body) in the z-axis direction, the scattered beam propagating along the y-axis is linearly polarized light. The electric field vector vibrates in the v plane and the vibration direction is parallel to the X axis. The sample placed on the y-axis is excited by polarized light, producing unpolarized fluorescent x-rays. Since the sample and the sample support do not generate scattered radiation in the X-axis direction, placing the detector on the x-axis can fully utilize the polarization effect and reduce the background caused by the elastic and inelastic scattering of x-rays.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Third, ultra-short optical design

    From the X-ray generator to the sample, the X-ray fluorescence emitted by the sample to the detector is called the light path. The shorter the distance traveled by the optical path is, the less interference will be caused. Skyray Instrument designed an ultra-short optical path technology to ensure the accuracy of light element detection results, and is particularly suitable for RoHS-compliant halogen-free instruction detection.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Fourth, precision machinery design

    The micro-level positioning, micro-scanning analysis, the point-to-point centering of the spatial micro-sized spot and the determination of the spatial micro-focus spot position have been truly achieved. A translation and rotation switching position device realizes position rotation switching in a small space, avoids the large space required for the linear motion and the common rotation movement, because the problem of lengthening of the optical path caused by the inability to fit is eliminated.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Five, no standard technology

    XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    Sixth, secondary target excitation technology

    XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    VII. Signal to Noise Enhancement Technology

    Skyray's unique SNR enhancement technology can effectively remove noise signal interference and minimize element detection limits.
    As shown in Figure SUPER XRF 1050, the determination of Pb in food can be as low as 0.59 ppm.

GC-MS6800 Detection of Phthalates in Electronic Information Products...

    VIII. XRF Core Technology (Intelligent Analysis Software)

    patented intelligent analysis software enables precise analysis of 80 elements, non-standard quantitative analysis, micro-analysis, thin film analysis, and advanced sub-spectral analysis.

Certificate of honor

The national Torch Program focuses on the high and new technology enterprises, the certification of heavy contract and credit enterprise, the confirmation certificate of measurement guarantee and the national high technology research and development plan (863 plan).:

国家火炬计划重点高新技术企业、重合同守信用企业认证、计量保证确认证书、国家高技术研究发展计划(863计划)-Jiangsu Skyray Instrument Co., Ltd.

ISO9001:2008 quality management system certification, ISO14001 environmental management system certificate, OHSAS 18001 occupational health and safety management health system, information security management system certification:

ISO9001:2008质量管理体系认证、ISO14001环境管理体系证书、OHSAS 18001 职业健康安全管理健康体系 、信息安全管理体系认证-Jiangsu Skyray Instrument Co., Ltd.

Practical patent certificate:

实用专利证书-Jiangsu Skyray Instrument Co., Ltd.

Standard formulation:

Jiangsu Skyray Instrument Co., Ltd.标准制定

Software copyright certificate:

软件著作权证书-Jiangsu Skyray Instrument Co., Ltd.

Other certificates:

Honor企业荣耀-Jiangsu Skyray Instrument Co., Ltd.
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CONTACT US

Jiangsu Skyray Instrument Co., Ltd.
SHENZHEN Skyray Instrument Co., Ltd.

hotline:800-9993-818
TEL:86 136 1622 3382
Address: 1888 Zhonghuayuan West Road, Kunshan City, Jiangsu Province/
深圳宝安区松岗芙蓉东路桃花源科技创新园22层

Jiangsu Skyray Instrument Co.,LTD.   苏ICP备11050632号   苏公网安备 32058302001500 号