性能优势
直读光谱仪OES1000采用光电倍增管(PMT)技术和独特光路设计使其具有优异性能,尤其对真空紫外谱线(涉及C、P、S、B、Sn等元素)、常量和痕量含量元素的检测有独特优势,是追求高性能测试用户的首选。
全天候工作,具有优异的稳定性和可靠性
样品测试速度快,单次测试过程少于40秒
软件可对测试结果自动判定牌号
仪器使用和维护简单、方便,对人员专业要求低
原厂安装分析程序,测试数据精确,适用合金牌号齐全
配置标准化样品可对仪器进行周期性校正
不使用化学试剂,测试过程安全、环保
技术性能及参数
1.分光室设计
帕邢-龙格装置,1米焦距
根据测试需求分为真空型(真空度≤3Pa)、空气型两种
恒温控制(32℃±0.1℃)
特殊材质铸造,保证光室形变小
2.最多安装通道 32
3.凹面光栅
刻线密度2160gr/mm
曲率半径998.8mm
逆线色散率0.47nm/mm
波长范围170-463nm
4.狭缝宽度
入射狭缝20μm,
出射狭缝为整体狭缝,宽度为35-75μm
5.光电倍增管
10级侧窗型,熔融石英或玻璃外壳;
6.分析时间
依样品种类而不同,一般少于40秒
7.激发光源
高能预火花光源(HEPS),放电频率100-900Hz,电极间距3-4mm
8.测光方式
采用光电倍增管检测器测光,光电倍增管负高压连续可调,传统的分段积分法
9.控制系统
采用FPGA技术控制整个仪器的工作状态
10.尺寸和重量
尺寸:1680(长)×1020(宽)×1150(高)mm
重量:约500kg
应用领域
金属材料元素含量测试是金属冶炼、铸造、加工以及机械行业的研发、生产控制、质量检验等相关工作的传统测试项目。
天瑞仪器直读光谱仪广泛应用于钢铁、有色金属材料元素含量分析,可快速、精确、稳定、同时测试几十种元素, 测试过程便捷、环保、低成本,满足工业研发、工艺控制、进料检验、产品分选等多方面的需求。
天瑞仪器直读光谱仪的快速测试使研发、生产过程和质量更可控,帮助用户提升产品的技术、质量水平;使相关流程加快,为用户创造明显的经济效益和环保效益。直读光谱仪已成为衡量企业技术和质量水平的标志性设备。
技术优势
全谱检测全面测试各种金属和元素
基于CCD检测器全谱测试技术,全面测试各种金属中元素的谱线,方便实现多基体、多元素的测试。
配置和补充测试基体、通道、分析程序极为方便,方便交货后在客户处补充测试元素、分析程序。
专业的测试方案
长期测试技术服务的积淀,天瑞仪器为钢铁、有色金属材料分析用户提供成熟的测试方案。
测试方案采用针对材料元素含量分类的分析程序,满足用户各类常见测试需求。
分析程序由原厂采用国际、国家标准样品校准,经专业仪器软件拟合、校正。
用户只需采用原厂配置少量标准化样品即可完成日常维护,不需购买大量制作分析程序的标准样品。
国际知名供应商提供核心部件
光谱色散元件——光栅由德国Zeiss制造,保证优异的光谱分辨能力
光谱检测器——高性能CCD由日本滨松Hamamatsu制造,确保谱线检测灵敏、低噪声
光学镜片——德国Zeiss制造,光纤——美国Agilent制造
光室真空系统
光室真空腔体经精密设计和加工,密闭性能优异,为光路提供优质的高真空环境。
因此真空泵启动时间和次数极少,电力消耗极少,更好保持光室清洁。
优秀的光室恒温系统
光室恒温腔体内配置反馈式加热装置和高效隔温层,有效保证光室内恒温。
由此抑制温度变化下机械件尺寸微弱变化导致的光路漂移。同时光电器件工作在恒温环境有助于性能的稳定。
天瑞仪器光谱仪厂家
天瑞仪器介绍
江苏天瑞仪器股份有限公司是具有自主知识产权的高科技企业,注册资本15392万。上市公司。
旗下拥有北京邦鑫伟业技术开发有限公司和深圳市天瑞仪器有限公司两家全资子公司。总部位于风景秀丽的江苏省昆山市阳澄湖畔。公司专业从事光谱、色谱、质谱等分析测试仪器及其软件的研发、生产和销售。
Why select Skyray Instruments?
First, the industry leader:
Listed on Shenzhen Stock Exchange in 2011(Code:300165),
Analytical instrument industry leader in the field
Skyray Instrument, as a leader in the domestic chemical analysis industry, specializes in the production of high-end analytical instruments such as spectrometers, chromatographs, and mass spectrometers. Mainly used in environmental protection and safety (electronics, electricity, toys and other consumer products industries, food safety, air, soil, water quality pollution detection, etc.), industrial production quality control (metallurgy, building materials, petroleum, chemical, precious metals, medical equipment, etc. ), minerals and resources (geology, mining), commodity inspections, quality inspections, and even human trace element testing and many other areas.The core patent technology is the first in the industry; the sales volume is the first in the industry; the product category is the first in the industry;
Second, the standard makers:
Skyray Instrument participated in drafting and formulating 18 national standards,
Industry standards, confident in the right to speak in the industry.
GBT 28020-2011 Ornaments Determination of harmful elements X-ray fluorescence spectroscopy
GBT 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
GBT 33352-2016 General requirements for screening of restricted substances in electrical and electronic products X-ray fluorescence spectroscopy
GB/T 25934.1-2010 High-Purity Gold Chemical Analysis Method Ethyl Acetate Extraction Separation ICP-AES Spectrometry Determination of Impurity Elements
GB/T 27730-2011 Determination of dimethyl fumarate in toy products Gas chromatography-mass spectrometry GC-MS method
GB/T 28020-2011 articles - Determination of harmful elements - X-ray fluorescence spectrometry
GBT 22788-2008 Determination of Total Lead in Coatings on Toys
GB/T 30419-2013 Determination of migrating elements in gallium arsenic, cadmium, chromium, lead, mercury selenium in toy materials Inductively coupled plasma atomic emission spectrometry
GB/T 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
JBT 12962.1-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 1: General Techniques
JBT 12962.2-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 2: Elemental Analyzers
JBT 12962.3-2016 Energy dispersive X-ray fluorescence spectrometer Part 3: Coating thickness analyzer
LS_T 6115-2016.4672 LST6115-2016 "Fastness determination of cadmium in rice by X-ray fluorescence spectrometry" standard
(Unfinished……)
Third, technology pioneers:
252 utility patents to fill domestic gaps and break the import monopoly
As of the end of 2017, Tianrui Instrument Company and its subsidiaries have obtained 252 patents authorized by the State Intellectual Property Office.
"Computer Software Copyright Registration Certificate" 91 items;
Of which 115 are invention patents,
80 utility model patents,
Appearance patent 57 items.
Fourth, service practitioners:
Do not forget the initial heart, with the customer with the fate, a total of growth.
Skyray customers include the General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China and the National Museum of China,
China National Center for Geoanalysis and Experiments, Chinese Academy of Geological Sciences, Changchun Institute of Opto-Mechanical Engineering, China Taier Laboratory,
Other government departments and well-known testing agencies,
And PetroChina, Sinopec, Huawei, Haier, Skyworth, Fanta, Meiling, Lite-On, TCL, LG, Midea, Samsung, China Test (CTI), Avionics, etc.
研发实力:
Analytical Testing Instrument Research Institute
Skyray Analytical Testing Instrument Research Institute has three centers, namely "analysis instrument research and development center", "physiochemical analysis and testing center" and "analysis and testing technology application development center."Tianrui Analytical Instruments Co., Ltd. recently formed a staff of 1 academician, 11 Ph.D., 13 senior engineers, 17 masters, and 50 undergraduate R&D personnel from famous universities.
Dr. Liu Zhaogui, specialist in special allowance of the State Council
Mr. Liu Zhaogui: graduate student in nuclear physics from Tsinghua University. It has been appraised as the outstanding entrepreneur of Jiangsu Province, the young and middle-aged experts who have outstanding contribution in Jiangsu Province, the first science and Technology Minister of Kunshan, and the national science and technology ministry "scientific and technological innovation and entrepreneurial talent". With the approval of the State Council, the special allowance of the State Council is enjoyed.
Dr. Yaodong Dong, Expert in X-Ray Fluorescence Spectroscopy
Dr. Yao graduated from the Department of Engineering Physics of Tsinghua University with a Ph.D. in nuclear electronics. He has been engaged in the development of analytical instruments for 26 years. He is mainly engaged in the research of X-ray fluorescence analysis technology and application technology, and he participated in the "Thirteenth Five-Year Plan" national key instrument technology research and development. Patent of "Spectrometer Grating 2D" patent, "X-ray fluorescence double crystal fixed element track spectrometer" patent and "X-ray fluorescence spectrum analyzer pyrolytic graphite crystal beam splitter" patent, and participated in the drafting of a number of national standards industry The standard is an authoritative expert in the X-ray fluorescence spectrometer industry in China.
Eight technical advantages:
First, FP basic parameter method
The FP (Basic Parameters) algorithm is an effective method for X-ray fluorescence spectrometry analysis. It can perform qualitative and quantitative analysis of the elemental components of the sample with little or no standard sample, and can also analyze the thickness of the coating or coating.It is well known that the biggest problem with X-ray fluorescence analysis is that elemental fluorescence intensity is affected by coexisting elements (matrix absorption and enhancement effects) and is not usually linear with content. The basic parameter method has already taken into account the matrix effect in the calculation of the spectrum, and the linear relationship between the calculated content and the known content can be obtained. Using a few known sample calibration algorithms to eliminate systematic errors can achieve accurate quantitative results.
Second, polarization secondary target excitation technology
The polarization secondary target excitation technology can remove the scattering background to the maximum extent, improve the signal to noise ratio, and reduce the detection limit of the detector. Assuming that the x-ray generated by the anode of the x-ray tube is non-polarized and is incident on the target (scattering body) in the z-axis direction, the scattered beam propagating along the y-axis is linearly polarized light. The electric field vector vibrates in the v plane and the vibration direction is parallel to the X axis. The sample placed on the y-axis is excited by polarized light, producing unpolarized fluorescent x-rays. Since the sample and the sample support do not generate scattered radiation in the X-axis direction, placing the detector on the x-axis can fully utilize the polarization effect and reduce the background caused by the elastic and inelastic scattering of x-rays.
Third, ultra-short optical design
From the X-ray generator to the sample, the X-ray fluorescence emitted by the sample to the detector is called the light path. The shorter the distance traveled by the optical path is, the less interference will be caused. Skyray Instrument designed an ultra-short optical path technology to ensure the accuracy of light element detection results, and is particularly suitable for RoHS-compliant halogen-free instruction detection.
Fourth, precision machinery design
The micro-level positioning, micro-scanning analysis, the point-to-point centering of the spatial micro-sized spot and the determination of the spatial micro-focus spot position have been truly achieved. A translation and rotation switching position device realizes position rotation switching in a small space, avoids the large space required for the linear motion and the common rotation movement, because the problem of lengthening of the optical path caused by the inability to fit is eliminated.
Five, no standard technology
XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.
Sixth, secondary target excitation technology
XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.
VII. Signal to Noise Enhancement Technology
Skyray's unique SNR enhancement technology can effectively remove noise signal interference and minimize element detection limits.
As shown in Figure SUPER XRF 1050, the determination of Pb in food can be as low as 0.59 ppm.
VIII. XRF Core Technology (Intelligent Analysis Software)
patented intelligent analysis software enables precise analysis of 80 elements, non-standard quantitative analysis, micro-analysis, thin film analysis, and advanced sub-spectral analysis.
Certificate of honor
The national Torch Program focuses on the high and new technology enterprises, the certification of heavy contract and credit enterprise, the confirmation certificate of measurement guarantee and the national high technology research and development plan (863 plan).:
ISO9001:2008 quality management system certification, ISO14001 environmental management system certificate, OHSAS 18001 occupational health and safety management health system, information security management system certification:
Practical patent certificate:
Standard formulation:
Software copyright certificate:
Other certificates: