1、ICP2000型电感耦合等离子体发射光谱仪用于测定各种物质(可溶解于盐酸、硝酸、氢氟酸等)中的常量、微量、痕量元素的含量。
2、仪器具有高效、抗干扰性强、自动化程度高、操作简便、稳定可靠、测试范围广、分析速度快、检出限低等特点。
3、广泛应用于稀土、地质、冶金、化工、环保、临床医药、石油制品、半导体、食品、生物样品、刑事科学、农业研究等各个领域。
仪器特点
可测元素70多种
分析速度快,一分钟可测5-8个元素
多元素同时分析,客户可以自由选择元素数量与安排测量顺序
检出限低,达到ppb量级,Ba甚至达到0.7ppb
线性动态范围宽,高达6个数量级,高低含量可以同时测量
分析成本低,一瓶氩气可以用8个小时
全反射消色差光学系统
采用凹面反射镜代替凸透镜作为光学聚焦元件,解决了不同元素焦点不同而引起的色差问题,同时提高光学系统效率。
波长范围宽
选择3600条刻线光栅,波长范围可达190nm-500nm
选择2400条刻线光栅,波长范围可达190nm-800nm
全自动化设计
自动化程度高,整台仪器除了电源开关,仪器所有功能都是通过计算机控制,可靠、安全、方便。
气体流量自动控制
进样系统中,载气、等离子气、辅气全部采用先进的质量流量控制器(MFC)来控制,具有流量连续可调、流量稳定等优点,确保了进样系统的稳定,为光源的稳定提供了坚强的保障。
先进的进样系统
进样系统高效、稳定,可配备国内外各种雾化器、雾化室,可以配备高盐雾化器,耐氢氟酸雾化器等,满足不同客户的需求。
自动进样器:选配天瑞自主研发的自动进样器,让测试操作更加省心省力。
稳定的废液排除系统
通过蠕动泵进行废液排除,确保进样量与废液排除速度一致,客户可以根据需要适当调节速度,确保进样系统稳定。
稳定先进的全固态射频电源
仪器采用的射频电源为天瑞仪器自主研发的全固态射频电源,具有体积小、效率高、输出功率稳定、带有各种保护功能等诸多优点,进一步提高了仪器的稳定性与安全性。
快速准确的全自动匹配功能
负载终端采用天瑞仪器自主研发的全自动匹配技术,具有匹配速度快、精度高等优点,确保了输出功率大限度的加到了负载上面,提高电源的使用效率,从而提高仪器的稳定性,并使得整个点火过程方便简单。
一键点火
配合天瑞的固态电源与自动匹配技术,ICP2060T完美的实现了一键点火功能。用户只需点点火按钮,仪器自动进行气体吹扫、气体流量检查、点火、匹配等诸多动作,并将信息实时传递给客户,让客户省心省事。
观察高度调节自动化
不同的元素有不同的优秀观察高度,客户可以根据经验或者比较,适当的通过软件调整火焰的观察高度,在优秀的位置得到好的测量效果。
强大的图形诊断功能
强大的图形诊断功能可以帮助客户充分的了解当前仪器的工作状态,并通过适当的参数设置来观察不同条件下仪器的运行状况,以把握优秀的测量条件。
多元素自动测量
选择需要测量的各个元素,设定好测量参数,一切交给仪器,后直接得到所有元素的测量结果,简单、省事。
强大的数据库管理
拥有几千条谱线,可以根据需要与爱好选择适当的谱线,避开可能存在的干扰,为您提供更多的选择,更合理的推荐,让测试变得更加专业与准确。
软件拥有自主知识产权,功能强大,操作人性化
ICP2060T 软件功能强大,具有中英文自动切换功能,可进行定性、定量分析;有数据再处理功能;自动计算元素含量,自动生成测试报告;具有数据筛选功能,剔除不想要的数据;数据库管理完善,可以自由保存与删除。
测试完毕后可以生成检测报告,检测报告内容可以根据用户需求选择,包括方法名称、仪器型号、元素、波长、强度、含量、相对标准偏差、单位、检测员、备注、校正人等,同时分析结果可以保存为pdf、word、excel等文件,方便用户分析。
软件界面设计人性化,简单明了,大大提高了分析效率。软件主界面集成软件的主要功能,包括控制等离子点火和灭火、仪器状态、分析参数、分析谱线、波长谱图显示、曲线拟合、数据处理、历史谱图、历史数据、用户管理等诸多功能。
产品规格与技术指标
体积:台式,1510mm×620mm×1200mm
固态电源
工作频率:40.68MHz
频率稳定性:<0.05%
匹配方式:软件匹配
输出功率:800W ~1200W
输出功率稳定性:≤0.2%
输出工作线圈内径25mm、3匝,配三同心外径20mm的石英炬管
同轴型喷雾器外径6mm;双筒型雾室外径35mm
扫描分光器
光路:Czerny turner型
焦距:1000mm
光栅规格:离子刻蚀全息光栅,刻线密度3600L/mm或2400L/mm;刻划面积(80×110)mm
分辨率:≤0.008nm(3600线光栅) ≤0.015nm(2400线光栅)
扫描波长范围:3600线光栅:(190~500) nm;2400线光栅:(190~800) nm
电子测量及控制电路
光电倍增管规格:R212/R928
光电倍增管负高压:(-50~-1000)V
光电倍增管电流测量范围:(10-12~10-4)A
信号采集:VF转换
计算机系统
主机:联想品牌电脑
显示器:17英寸液晶显示器
打印机:Canon喷墨打印机
整机技术指标
扫描波长范围:190nm~500nm(3600L/mm光栅),190nm~800nm(2400L/mm光栅);
测量范围
a.液体含量:0.01ppm-几千ppm
b.固体含量:0.001%------70%
重复性:(即短期稳定度)相对标准偏差RSD≤2.0% ;
稳定性:相对标准偏差RSD≤2%;
测试速度:5-8元素/每分钟
典型元素检出限(μg/L):
元素 | La | Ce | Pr | Nd | Sm | Eu | Gd | Tb |
波长(nm) | 408.672 | 413.765 | 414.311 | 401.225 | 360.946 | 381.967 | 342.247 | 350.917 |
检出限 | <3.0 | <5.0 | <5.0 | <5.0 | < 10.0 | < 1.0 | <10.0 | < 3.0 |
元素 | Dy | Ho | Er | Tm | Yb | Lu | Y | Sc |
波长(nm) | 353.170 | 345.600 | 337.271 | 313.126 | 369.419 | 261.541 | 371.030 | 335.373 |
检出限 | <3.0 | <3.0 | <3.0 | <3.0 | <1.0 | <3.0 | <1.0 | <1.0 |
元素 | Ta | Nb | Mn | Mg | B | Zn | Co | Si |
波长(nm) | 226.230 | 313.340 | 257.610 | 279.553 | 249.773 | 13.856 | 228.616 | 251.611 |
检出限 | <5.0 | <5.0 | <3.0 | <1.0 | <10.0 | <3.0 | <3.0 | <10.0 |
元素 | Ni | Cd | Fe | Ca | Mo | V | Be | Ti |
波长(nm) | 232.003 | 226.502 | 239.562 | 393.366 | 281.615 | 310.230 | 313.041 | 334.941 |
检出限 | <5.0 | <3.0 | <3.0 | <1.0 | <5.0 | <5.0 | <1.0 | <3.0 |
元素 | Cu | Cr | Al | Zr | Ag | Sr | Au | Pt |
波长(nm) | 324.754 | 267.716 | 396.152 | 343.823 | 328.068 | 407.771 | 242.795 | 265.945 |
检出限 | <3.0 | & |
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Why select Skyray Instruments?
First, the industry leader:
Listed on Shenzhen Stock Exchange in 2011(Code:300165),
Analytical instrument industry leader in the field
Skyray Instrument, as a leader in the domestic chemical analysis industry, specializes in the production of high-end analytical instruments such as spectrometers, chromatographs, and mass spectrometers. Mainly used in environmental protection and safety (electronics, electricity, toys and other consumer products industries, food safety, air, soil, water quality pollution detection, etc.), industrial production quality control (metallurgy, building materials, petroleum, chemical, precious metals, medical equipment, etc. ), minerals and resources (geology, mining), commodity inspections, quality inspections, and even human trace element testing and many other areas.The core patent technology is the first in the industry; the sales volume is the first in the industry; the product category is the first in the industry;
Second, the standard makers:
Skyray Instrument participated in drafting and formulating 18 national standards,
Industry standards, confident in the right to speak in the industry.
GBT 28020-2011 Ornaments Determination of harmful elements X-ray fluorescence spectroscopy
GBT 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
GBT 33352-2016 General requirements for screening of restricted substances in electrical and electronic products X-ray fluorescence spectroscopy
GB/T 25934.1-2010 High-Purity Gold Chemical Analysis Method Ethyl Acetate Extraction Separation ICP-AES Spectrometry Determination of Impurity Elements
GB/T 27730-2011 Determination of dimethyl fumarate in toy products Gas chromatography-mass spectrometry GC-MS method
GB/T 28020-2011 articles - Determination of harmful elements - X-ray fluorescence spectrometry
GBT 22788-2008 Determination of Total Lead in Coatings on Toys
GB/T 30419-2013 Determination of migrating elements in gallium arsenic, cadmium, chromium, lead, mercury selenium in toy materials Inductively coupled plasma atomic emission spectrometry
GB/T 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
JBT 12962.1-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 1: General Techniques
JBT 12962.2-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 2: Elemental Analyzers
JBT 12962.3-2016 Energy dispersive X-ray fluorescence spectrometer Part 3: Coating thickness analyzer
LS_T 6115-2016.4672 LST6115-2016 "Fastness determination of cadmium in rice by X-ray fluorescence spectrometry" standard
(Unfinished……)
Third, technology pioneers:
252 utility patents to fill domestic gaps and break the import monopoly
As of the end of 2017, Tianrui Instrument Company and its subsidiaries have obtained 252 patents authorized by the State Intellectual Property Office.
"Computer Software Copyright Registration Certificate" 91 items;
Of which 115 are invention patents,
80 utility model patents,
Appearance patent 57 items.
Fourth, service practitioners:
Do not forget the initial heart, with the customer with the fate, a total of growth.
Skyray customers include the General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China and the National Museum of China,
China National Center for Geoanalysis and Experiments, Chinese Academy of Geological Sciences, Changchun Institute of Opto-Mechanical Engineering, China Taier Laboratory,
Other government departments and well-known testing agencies,
And PetroChina, Sinopec, Huawei, Haier, Skyworth, Fanta, Meiling, Lite-On, TCL, LG, Midea, Samsung, China Test (CTI), Avionics, etc.
研发实力:
Analytical Testing Instrument Research Institute
Skyray Analytical Testing Instrument Research Institute has three centers, namely "analysis instrument research and development center", "physiochemical analysis and testing center" and "analysis and testing technology application development center."Tianrui Analytical Instruments Co., Ltd. recently formed a staff of 1 academician, 11 Ph.D., 13 senior engineers, 17 masters, and 50 undergraduate R&D personnel from famous universities.
Dr. Liu Zhaogui, specialist in special allowance of the State Council
Mr. Liu Zhaogui: graduate student in nuclear physics from Tsinghua University. It has been appraised as the outstanding entrepreneur of Jiangsu Province, the young and middle-aged experts who have outstanding contribution in Jiangsu Province, the first science and Technology Minister of Kunshan, and the national science and technology ministry "scientific and technological innovation and entrepreneurial talent". With the approval of the State Council, the special allowance of the State Council is enjoyed.
Dr. Yaodong Dong, Expert in X-Ray Fluorescence Spectroscopy
Dr. Yao graduated from the Department of Engineering Physics of Tsinghua University with a Ph.D. in nuclear electronics. He has been engaged in the development of analytical instruments for 26 years. He is mainly engaged in the research of X-ray fluorescence analysis technology and application technology, and he participated in the "Thirteenth Five-Year Plan" national key instrument technology research and development. Patent of "Spectrometer Grating 2D" patent, "X-ray fluorescence double crystal fixed element track spectrometer" patent and "X-ray fluorescence spectrum analyzer pyrolytic graphite crystal beam splitter" patent, and participated in the drafting of a number of national standards industry The standard is an authoritative expert in the X-ray fluorescence spectrometer industry in China.
Eight technical advantages:
First, FP basic parameter method
The FP (Basic Parameters) algorithm is an effective method for X-ray fluorescence spectrometry analysis. It can perform qualitative and quantitative analysis of the elemental components of the sample with little or no standard sample, and can also analyze the thickness of the coating or coating.It is well known that the biggest problem with X-ray fluorescence analysis is that elemental fluorescence intensity is affected by coexisting elements (matrix absorption and enhancement effects) and is not usually linear with content. The basic parameter method has already taken into account the matrix effect in the calculation of the spectrum, and the linear relationship between the calculated content and the known content can be obtained. Using a few known sample calibration algorithms to eliminate systematic errors can achieve accurate quantitative results.
Second, polarization secondary target excitation technology
The polarization secondary target excitation technology can remove the scattering background to the maximum extent, improve the signal to noise ratio, and reduce the detection limit of the detector. Assuming that the x-ray generated by the anode of the x-ray tube is non-polarized and is incident on the target (scattering body) in the z-axis direction, the scattered beam propagating along the y-axis is linearly polarized light. The electric field vector vibrates in the v plane and the vibration direction is parallel to the X axis. The sample placed on the y-axis is excited by polarized light, producing unpolarized fluorescent x-rays. Since the sample and the sample support do not generate scattered radiation in the X-axis direction, placing the detector on the x-axis can fully utilize the polarization effect and reduce the background caused by the elastic and inelastic scattering of x-rays.
Third, ultra-short optical design
From the X-ray generator to the sample, the X-ray fluorescence emitted by the sample to the detector is called the light path. The shorter the distance traveled by the optical path is, the less interference will be caused. Skyray Instrument designed an ultra-short optical path technology to ensure the accuracy of light element detection results, and is particularly suitable for RoHS-compliant halogen-free instruction detection.
Fourth, precision machinery design
The micro-level positioning, micro-scanning analysis, the point-to-point centering of the spatial micro-sized spot and the determination of the spatial micro-focus spot position have been truly achieved. A translation and rotation switching position device realizes position rotation switching in a small space, avoids the large space required for the linear motion and the common rotation movement, because the problem of lengthening of the optical path caused by the inability to fit is eliminated.
Five, no standard technology
XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.
Sixth, secondary target excitation technology
XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.
VII. Signal to Noise Enhancement Technology
Skyray's unique SNR enhancement technology can effectively remove noise signal interference and minimize element detection limits.
As shown in Figure SUPER XRF 1050, the determination of Pb in food can be as low as 0.59 ppm.
VIII. XRF Core Technology (Intelligent Analysis Software)
patented intelligent analysis software enables precise analysis of 80 elements, non-standard quantitative analysis, micro-analysis, thin film analysis, and advanced sub-spectral analysis.
Certificate of honor
The national Torch Program focuses on the high and new technology enterprises, the certification of heavy contract and credit enterprise, the confirmation certificate of measurement guarantee and the national high technology research and development plan (863 plan).:
ISO9001:2008 quality management system certification, ISO14001 environmental management system certificate, OHSAS 18001 occupational health and safety management health system, information security management system certification:
Practical patent certificate:
Standard formulation:
Software copyright certificate:
Other certificates: