Stock code:300165

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Jiangsu Skyray Instrument Co., Ltd.
Shenzhen Skyray Instrument Co., Ltd.

TEL+86 138 6264 8316

hotline+86 138 6264 8316

E-mailrohsxrf@126.com

addressNo. 1888, Zhonghuayuan West Road, Kunshan City, Jiangsu Province, 22/F, Taohuayuan Science and Technology Innovation Park, Furong East Road, Songgang, Bao'an District, Shenzhen, China

Inductively coupled plasma... HOME >> PRODUCT >> Inductively coupled plasma emission spectrometry ICP

Jiangsu Skyray Instrument Co., Ltd.-ICP 3000

Inductively coupled plasma emission...

ICP 3000

电感耦合等离子体发射光谱仪

 TEL:
  800-9993-818
  +86 138 0228 4651

 ICP 3000  Product Details

产品说明、技术参数及配置

ICP-3000电感耦合等离子体发射光谱仪是天瑞仪器公司经多年技术积累开发出的一款性能优异的全谱直读型光谱仪,用于测定不同物质(可溶解于盐酸、硝酸、氢氟酸等)中的微量、痕量元素含量。自动化程度高,操作简便,稳定可靠。目前仪器广泛应用于稀土、地质、冶金、化工、环保、临床医药、石油制品、半导体、食品、生物样品、刑事科学、农业研究等各个领域。

性能优势

全自动化设计
整台仪器除了电源开关,仪器所有功能都通过计算机控制,可靠、安全、方便。

蠕动泵
蠕动泵为十二转子四通道全自动设计,蠕动泵转速可根据需求流量设置调节;通过蠕动泵平稳进样和排除废液,确保进样速度与废液排除速度一致,客户可以根据需要适当调节速度,确保进样系统稳定。

气体流量自动控制
进样系统中,载气、等离子气、辅气均采用先进的质量流量控制器(MFC)来控制,具有流量连续可调、流量稳定等优点,确保了进样系统的稳定,为光源的稳定奠定了坚实的基础。

稳定先进的全固态射频电源
仪器采用的射频电源为天瑞仪器自主研发的全固态射频电源,具有体积小、效率高、输出功率稳定、带有各种保护功能等诸多优点,进一步提高了仪器的稳定性与安全性。

快速准确的全自动匹配功能
负载终端采用天瑞仪器自主研发的全自动匹配技术,具有匹配速度快、精度高等优点,确保了输出功率最大限度地加予负载,提高了电源的使用效率,从而提高仪器的稳定性,并使得整个点火过程简单方便。

先进的进样系统
进样系统高效、稳定,可配备国内外各种雾化器、雾化室,可以配备高盐雾化器、耐氢氟雾化器等,满足客户的各种需求;同时天瑞自主研发的自动进样器让测试操作更加便捷,进一步提高测试效率。

独特精密的光学系统
采用中阶梯光栅-棱镜交叉色散方式,专业的光学优化设计使得光通量最大化的同时保证了优异的光谱分辨率;无任何移动光学元件,保证了良好的长期稳定性;超低杂散光设计配合独特的光学设计,大大降低了背景光的干扰,进一步提高检出限;高效的氮气分布式吹扫光室配合高品质的光学元件保证了深紫外区特别是P、S、As等元素的测量。

精准的波长定位
智能精确的自动波长校准算法,无需进行额外的谱峰校正即可进行测量,保证准确测量的同时节约大量的标液和测量时间。

性能优异的探测器
采用大尺寸CID探测器,先进、成熟、稳定;大靶面尺寸,百万级像素;165-900nm范围连续覆盖,一次曝光,全谱显示;非破坏性读取(NDRO) 功能,改善了弱分析线的信噪比,提高了结果的准确性,并且数据采集与分析均优于CCD; 极佳的线性动态范围和与生俱来的抗溢出功能确保任意强弱的谱线可在一次曝光内测量并进行分析,同时为方法选择理想波长提供了灵活性(可选第二、第三或更次灵敏线来排除干扰)。

超快的测试速度
各分析谱线可以在曝光时间内设置任意合适的积分时段来实现测量的最优化;可以一次曝光读出所有分析谱线的强度积分值加快分析速度;还可以指定谱线独立读出,读出时间不超过2ms。

强大的软件分析功能
软件操作方便、直观,具有定性、半定量、定量分析功能,具有仪器诊断优化功能,灵活的全谱研究功能,强大的离线再处理功能,具有科学智能的背景校正、去除干扰的算法功能,让测试变得更加专业与准确。

技术参数

射频发生器技术指标
输入电源:交流220V,电流20A
输出功率:700~1600W
调节精度:2W
频率稳定性:<0.05%
输出功率稳定性:<0.1%
匹配方式:自动匹配
电磁场泄漏辐射强度:距机箱30cm处电场强度E:<0.5V/m

进样装置技术指标
输出工作线圈:内径25mm、3匝
三同心石英炬管:外径20mm;根据中心通道大小有多种型号可选
高效进口雾化器:同心型雾化器,外径6mm ;多型号可选,高盐、耐HF等
雾化室:双筒型雾化室,可以选配旋流式雾化室,外径57.2mm
蠕动泵:十二转子四通道,转速可根据需求流量设置调节(即根据进样速度设定,直观,准确)
总氩气消耗量:氩气总消耗量小于14L/min
氩气流量计和载气压力表规格:1.等离子气流量计(100~1000)L/h (1.6~16L/min)
2.辅助气流量计(6~60)L/h (0.1~1L/min)
3.载气流量计(6~60)L/h (0.1~1L/min)
4.载气稳压阀(0.2MPa)
5.冷却水:水温20~25℃ 流量>5L/min 水压>0.1MPa

分光器技术指标
光栅:中阶梯光栅,52.67 lp/mm,64闪耀角,采用德国肖特公司热膨胀系数接近于零的
Zerodur材料做基底,性能更出众
棱镜:超纯康宁紫外熔融石英,在170nm处内透过率99.6%
波长范围:165nm~900nm
焦距:430mm
数值孔径:F/8,超高的光通量保证仪器的检出限和灵敏度
分辨率:<0.0068nm@200nm
杂散光:10000ppmCa 溶液在As189.042nm处的等效背景浓度<2ppm
光室:精密恒温,35±0.1℃
分布式氮气吹扫,正常吹扫2L/min,快速吹扫4L/min

检测装置技术指标
检测器类型:电荷注入式检测器(CID)
靶面尺寸:27.6mm×27.6mm,1024×1024寻址检测单元
读取方式:非破坏性读取(NDRO) ,全幅读取(FF)和任意读取积分(RAI)
线性动态范围:108
波长响应范围:165nm~1000nm
电子快门:单独设置各谱线的积分时间;可指定谱线独立读出,读出时间<2ms
量子效率:无任何镀膜,200nm紫外区可达35%以上
检测器冷却:高效三级半导体制冷,制冷温度-45℃

仪器技术指标
观测方式:垂直观测
液体含量:0.01ppm~几千ppm
固体含量:0.001%~70%
重复性:(即短期稳定度)相对标准偏差RSD<0.5%
稳定性:相对标准偏差RSD<1% @2小时
测试速度:单个谱线CID读出时间仅需2ms,一分钟内可实现所有元素的测量
元素检出限(μg/L):大部分元素1ppb~10ppb
仪器尺寸:台式1300mm*840mm*740mm

应用领域
1.硅工业:磁性材料加工行业
2.冶金工业:可分析对金属材料质量影响很大的As、Bi、Pb、Sb、Sn等杂质元素
3.水质分析:可检测水质污染的八大重金属等元素
4.地质、矿石分析:岩石样品中Ca、Mg、Na、Fe、Cu、Mn、Zn、Co、Ni、Au、Ag等元素的测定
5.石油化工和轻工领域的应用:测试原油中的30多种元素,主要有Fe、Na、Mg、Ni、V、Ca、Pb、Mo、Mn、Cr、Co、Ba、As等
6.医疗、卫生、农业环保、商品、食品质量检测


Why select Skyray Instruments?

ICP 3000

    First, the industry leader:

    Listed on Shenzhen Stock Exchange in 2011(Code:300165)
    Analytical instrument industry leader in the field

    Skyray Instrument, as a leader in the domestic chemical analysis industry, specializes in the production of high-end analytical instruments such as spectrometers, chromatographs, and mass spectrometers. Mainly used in environmental protection and safety (electronics, electricity, toys and other consumer products industries, food safety, air, soil, water quality pollution detection, etc.), industrial production quality control (metallurgy, building materials, petroleum, chemical, precious metals, medical equipment, etc. ), minerals and resources (geology, mining), commodity inspections, quality inspections, and even human trace element testing and many other areas.The core patent technology is the first in the industry; the sales volume is the first in the industry; the product category is the first in the industry;

ICP 3000

    Second, the standard makers:

    Skyray Instrument participated in drafting and formulating 18 national standards, Industry standards, confident in the right to speak in the industry.

    GBT 28020-2011 Ornaments Determination of harmful elements X-ray fluorescence spectroscopy
    GBT 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
    GBT 33352-2016 General requirements for screening of restricted substances in electrical and electronic products X-ray fluorescence spectroscopy
    GB/T 25934.1-2010 High-Purity Gold Chemical Analysis Method Ethyl Acetate Extraction Separation ICP-AES Spectrometry Determination of Impurity Elements
    GB/T 27730-2011 Determination of dimethyl fumarate in toy products Gas chromatography-mass spectrometry GC-MS method
    GB/T 28020-2011 articles - Determination of harmful elements - X-ray fluorescence spectrometry
    GBT 22788-2008 Determination of Total Lead in Coatings on Toys
    GB/T 30419-2013 Determination of migrating elements in gallium arsenic, cadmium, chromium, lead, mercury selenium in toy materials Inductively coupled plasma atomic emission spectrometry
    GB/T 31364-2015 Energy dispersive X-ray fluorescence spectrometer main performance test method
    JBT 12962.1-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 1: General Techniques
    JBT 12962.2-2016 Energy Dispersive X-Ray Fluorescence Spectrometer Part 2: Elemental Analyzers
    JBT 12962.3-2016 Energy dispersive X-ray fluorescence spectrometer Part 3: Coating thickness analyzer
    LS_T 6115-2016.4672 LST6115-2016 "Fastness determination of cadmium in rice by X-ray fluorescence spectrometry" standard
    (Unfinished……)

ICP 3000

    Third, technology pioneers:

    252 utility patents to fill domestic gaps and break the import monopoly

    As of the end of 2017, Tianrui Instrument Company and its subsidiaries have obtained 252 patents authorized by the State Intellectual Property Office.
    "Computer Software Copyright Registration Certificate" 91 items;
    Of which 115 are invention patents,
    80 utility model patents,
    Appearance patent 57 items.

ICP 3000

    Fourth, service practitioners:

    Do not forget the initial heart, with the customer with the fate, a total of growth.

    Skyray customers include the General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China and the National Museum of China,
    China National Center for Geoanalysis and Experiments, Chinese Academy of Geological Sciences, Changchun Institute of Opto-Mechanical Engineering, China Taier Laboratory,
    Other government departments and well-known testing agencies,
    And PetroChina, Sinopec, Huawei, Haier, Skyworth, Fanta, Meiling, Lite-On, TCL, LG, Midea, Samsung, China Test (CTI), Avionics, etc.

研发实力:

ICP 3000

    Analytical Testing Instrument Research Institute

    Skyray Analytical Testing Instrument Research Institute has three centers, namely "analysis instrument research and development center", "physiochemical analysis and testing center" and "analysis and testing technology application development center."Tianrui Analytical Instruments Co., Ltd. recently formed a staff of 1 academician, 11 Ph.D., 13 senior engineers, 17 masters, and 50 undergraduate R&D personnel from famous universities.

ICP 3000

    Dr. Liu Zhaogui, specialist in special allowance of the State Council

    Mr. Liu Zhaogui: graduate student in nuclear physics from Tsinghua University. It has been appraised as the outstanding entrepreneur of Jiangsu Province, the young and middle-aged experts who have outstanding contribution in Jiangsu Province, the first science and Technology Minister of Kunshan, and the national science and technology ministry "scientific and technological innovation and entrepreneurial talent". With the approval of the State Council, the special allowance of the State Council is enjoyed.

ICP 3000

    Dr. Yaodong Dong, Expert in X-Ray Fluorescence Spectroscopy

    Dr. Yao graduated from the Department of Engineering Physics of Tsinghua University with a Ph.D. in nuclear electronics. He has been engaged in the development of analytical instruments for 26 years. He is mainly engaged in the research of X-ray fluorescence analysis technology and application technology, and he participated in the "Thirteenth Five-Year Plan" national key instrument technology research and development. Patent of "Spectrometer Grating 2D" patent, "X-ray fluorescence double crystal fixed element track spectrometer" patent and "X-ray fluorescence spectrum analyzer pyrolytic graphite crystal beam splitter" patent, and participated in the drafting of a number of national standards industry The standard is an authoritative expert in the X-ray fluorescence spectrometer industry in China.

Eight technical advantages:

ICP 3000

    First, FP basic parameter method

    The FP (Basic Parameters) algorithm is an effective method for X-ray fluorescence spectrometry analysis. It can perform qualitative and quantitative analysis of the elemental components of the sample with little or no standard sample, and can also analyze the thickness of the coating or coating.It is well known that the biggest problem with X-ray fluorescence analysis is that elemental fluorescence intensity is affected by coexisting elements (matrix absorption and enhancement effects) and is not usually linear with content. The basic parameter method has already taken into account the matrix effect in the calculation of the spectrum, and the linear relationship between the calculated content and the known content can be obtained. Using a few known sample calibration algorithms to eliminate systematic errors can achieve accurate quantitative results.

ICP 3000

    Second, polarization secondary target excitation technology

    The polarization secondary target excitation technology can remove the scattering background to the maximum extent, improve the signal to noise ratio, and reduce the detection limit of the detector. Assuming that the x-ray generated by the anode of the x-ray tube is non-polarized and is incident on the target (scattering body) in the z-axis direction, the scattered beam propagating along the y-axis is linearly polarized light. The electric field vector vibrates in the v plane and the vibration direction is parallel to the X axis. The sample placed on the y-axis is excited by polarized light, producing unpolarized fluorescent x-rays. Since the sample and the sample support do not generate scattered radiation in the X-axis direction, placing the detector on the x-axis can fully utilize the polarization effect and reduce the background caused by the elastic and inelastic scattering of x-rays.

ICP 3000

    Third, ultra-short optical design

    From the X-ray generator to the sample, the X-ray fluorescence emitted by the sample to the detector is called the light path. The shorter the distance traveled by the optical path is, the less interference will be caused. Skyray Instrument designed an ultra-short optical path technology to ensure the accuracy of light element detection results, and is particularly suitable for RoHS-compliant halogen-free instruction detection.

ICP 3000

    Fourth, precision machinery design

    The micro-level positioning, micro-scanning analysis, the point-to-point centering of the spatial micro-sized spot and the determination of the spatial micro-focus spot position have been truly achieved. A translation and rotation switching position device realizes position rotation switching in a small space, avoids the large space required for the linear motion and the common rotation movement, because the problem of lengthening of the optical path caused by the inability to fit is eliminated.

ICP 3000

    Five, no standard technology

    XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.

ICP 3000

    Sixth, secondary target excitation technology

    XRF test and analysis instruments are generally used for the comparison test of standard samples, which are subject to the quality of the standard samples during the test. Tianrui Instrument's original non-standard technology can carry out all-element analysis without standard samples, leading the development trend and trend of the industry.

ICP 3000

    VII. Signal to Noise Enhancement Technology

    Skyray's unique SNR enhancement technology can effectively remove noise signal interference and minimize element detection limits.
    As shown in Figure SUPER XRF 1050, the determination of Pb in food can be as low as 0.59 ppm.

ICP 3000

    VIII. XRF Core Technology (Intelligent Analysis Software)

    patented intelligent analysis software enables precise analysis of 80 elements, non-standard quantitative analysis, micro-analysis, thin film analysis, and advanced sub-spectral analysis.

Certificate of honor

The national Torch Program focuses on the high and new technology enterprises, the certification of heavy contract and credit enterprise, the confirmation certificate of measurement guarantee and the national high technology research and development plan (863 plan).:

国家火炬计划重点高新技术企业、重合同守信用企业认证、计量保证确认证书、国家高技术研究发展计划(863计划)-Jiangsu Skyray Instrument Co., Ltd.

ISO9001:2008 quality management system certification, ISO14001 environmental management system certificate, OHSAS 18001 occupational health and safety management health system, information security management system certification:

ISO9001:2008质量管理体系认证、ISO14001环境管理体系证书、OHSAS 18001 职业健康安全管理健康体系 、信息安全管理体系认证-Jiangsu Skyray Instrument Co., Ltd.

Practical patent certificate:

实用专利证书-Jiangsu Skyray Instrument Co., Ltd.

Standard formulation:

Jiangsu Skyray Instrument Co., Ltd.标准制定

Software copyright certificate:

软件著作权证书-Jiangsu Skyray Instrument Co., Ltd.

Other certificates:

Honor企业荣耀-Jiangsu Skyray Instrument Co., Ltd.
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Jiangsu Skyray Instrument Co., Ltd.
SHENZHEN Skyray Instrument Co., Ltd.

hotline:800-9993-818
TEL:86 136 1622 3382
Address: 1888 Zhonghuayuan West Road, Kunshan City, Jiangsu Province/
深圳宝安区松岗芙蓉东路桃花源科技创新园22层

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